Stainless Steel Sample Loops
These high quality stainless steel sample loops have burr-free, square-cut ends to ensure a flush connection to valve ports. The size designations of loops are nominal. The actual volumes can differ from the theoretical designations because the ID tolerance varies depending on the tubing tolerance of the metal tubing bore. Accuracy of large metal loops (1.0 mm, 0.040” bore) is about ±5%, intermediate loops (0.5 mm, 0.020” bore) ±10%, and small loops (0.2 mm, 0.007” bore) ±30%. Since both standards and unknowns are usually analyzed using the same sample loop, knowledge of the actual, accurate volume is rarely needed. If the sample loop volume must be known, it is best to calibrate the loop in place on the valve so the flow passages in the valve are also taken into account. An alternative to calibration is to use a dual mode injector and partial-filling method of loading. See the “Sample Loop Loading” Application Note on page 133. Model 7725 Injector loops are not interchangeable with loops for the model 7125. The port angle for the 7725 is 30° whereas the port angle for the 7125 is 20° requiring the loops to have a different shape. Model 8125 Micro-Scale Sample Injector requires special loops in the 5.0 µL to 50 µL range. The 8125 sample loops are made with 0.5 mm (0.020”) OD tubing
Stainless Steel Sample Loops
How to Properly Install Sample Loops: Stainless Steel
Stainless steel sample loops are supplied
with fittings that are not swaged onto
the tube. It is important that the loop be
completely bottomed in the injector port
before the ferrule is swaged onto the tube.
The depth of the tubing holes may vary
slightly from port to port and from valve
to valve. A fitting made up in one port
may leave a small cavity in another port.
The cavity causes high dispersion and
peak distortion such as fronting, tailing,
or broadening. It is good practice to label
loop ends so they will be replaced in the
same, respective ports that were used
in swaging the ferrules. Hint: swaging
ferrules separately on each side, into
each respective valve port makes loop
installation easier.
등록된 상품이 없습니다.